KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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KBS30-2 - N-alkylation with KBS29 #116

Closed KlementineJBS closed 6 months ago

KlementineJBS commented 11 months ago

Link to HIRAC and master page.

Previous attempt is #58

KBS30 - Generic alkylation of 1,x-diaminoalkane with naphthalene-triazole pendant (updated).docx

Reaction scheme

KBS30 - alkylation of 1,x-diaminoalkane with naphthalene-triazole pendant group

KlementineJBS commented 11 months ago

Plan:

Use all of #63 (~ 1.0 g, 3.47 mmol).

Working backwards using 2.2 equiv. of the bromo-triazole-naphthyl group this means I need 1.58 mmol 1,6-diaminohexane = 183.19 mg.

KlementineJBS commented 11 months ago

LRMS

KBS30-2 crude.pdf KBS30-2 crude.d.zip

KlementineJBS commented 11 months ago

PXL_20230713_045019001.MP.jpg

PXL_20230713_045939758.jpg