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KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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KBS37-2 - Synthesis of 2-acetyl-quinoline #137

Closed KlementineJBS closed 1 year ago

KlementineJBS commented 1 year ago

Link to HIRAC.

KBS37 - Synthesis of 2-acetylquinoline .docx

Previous attempt was #118

Reaction scheme

KBS37 - Synthesis of 2-acetyl-quinoline

Outcome

857.6 mg (5.01 mmol, 64%)

KlementineJBS commented 1 year ago

25.08.23

  1. Dissolved SM (1.89567 g, 7.79 mmol) in 1,4-dioxane (19 mL)
  2. Added HCl (1 M, 19 mL)
  3. Left stirring at 100 C overnight
KlementineJBS commented 1 year ago

Workup as in #118

Empty vial: 15.7309 Full vial: 16.5885 Mass: 857.6 mg (5.01 mmol, 64%)

KlementineJBS commented 1 year ago

LRMS

KBS37-2 cr.pdf KBS37-2 cr.d.zip

KlementineJBS commented 1 year ago

H NMR

KBS37-2 2nd extract_1.zip KBS37-2 cr_1.zip KBS37-2 cr.pdf