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KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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2023_SSP_8D - Purification of student-synthesised material #141

Closed KlementineJBS closed 1 month ago

KlementineJBS commented 9 months ago

Reaction scheme

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KlementineJBS commented 9 months ago

LRMS

319.14 [M+H]+, 341.10 [M+Na]+, 317.08 [M-H]-.

2023_SSP_8D.pdf 2023_SSP_8D.d.zip

KlementineJBS commented 9 months ago

Column

F6-9 vial: 15.7133 Full vial: 15.9010 Mass: 187.7 mg

F13-20 vial: 15.7898 Full vial: 15.7993 Mass: 9.5 mg

LRMS

2023_SSP_8D F6-9.pdf 2023_SSP_8D F6-9.d.zip 2023_SSP_8D F13-20.d.zip 2023_SSP_8D F13-20.pdf

KlementineJBS commented 9 months ago

HPLC

Crude - purity = 47.37%

image

F6-9 - purity = 82.10%

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