search

KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
2 stars 0 forks source link

KBS45 - master page #167

Closed KlementineJBS closed 5 days ago

KlementineJBS commented 6 months ago

Link to HIRAC and master page.

KBS43 - Nosyl protection of linear diamine .docx

Reaction scheme

KBS43 - Nosyl protection of linear amines

KlementineJBS commented 6 months ago

Attempts

Identifier Link Yield Further info
1 #163 818 mg, 88% chloroform workup, not easily soluble
2 #168 1.615 g, 45% used THF as solvent
KlementineJBS commented 6 months ago

Notes

Have been using nosyl chloride borrowed from Macerlean group, and checked purity before use.