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KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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KBS48 (pooled) - purification #194

Closed KlementineJBS closed 2 months ago

KlementineJBS commented 2 months ago

KBS48 - Mitsunobu on linear amines

KlementineJBS commented 2 months ago

Was purifying leftover samples from KBS48-1 and KBS48-2 that contained bis product + DIAD. Combined mass of crude was 180 mg.

KlementineJBS commented 2 months ago

Column conditions

Results

Fractions Vial tare (g) Mass (mg) Substance
1-35 15.6117 40.8 product
36-65 15.6391 61 product
66-70 15.7917 - -
71-93 15.8061 48 likely PPh3O
94-98 15.5448 - appears to be PPh3O
KlementineJBS commented 2 months ago

H NMR

KBS48.pdf

nmr300_20240418_KBS48 F36-65_1 (1).zip nmr300_20240418_KBS48 F1-35_1 (1).zip nmr300_20240419_KBS48 F94-98_1.zip