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KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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KBS52-2 - Nosyl deprotection of KBS51 #195

Open KlementineJBS opened 2 months ago

KlementineJBS commented 2 months ago

Link to HIRAC and master page #186

Reaction scheme

image

KlementineJBS commented 2 months ago

24.04.24

Protocol as usual. 55 mg of KBS52-1 (mixture of materials), 0.3 mmol 2-mercaptoethanol (23 mg, 21 uL), 0.6 mmol K2CO3 (85 mg) and 2 mL DMF

Heated to 140 C from ~11 am.

KlementineJBS commented 2 months ago

LRMS of crude RM

KBS52-2 RM.d.zip KBS52-2 RM.pdf