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KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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Breaking Good SSP compounds 2022 - 8B #35

Closed KlementineJBS closed 1 year ago

KlementineJBS commented 2 years ago

image

NMR

BG_8B pure_1.zip

BG_8B pure processed.pdf

Looks good, minor solvent impurities between 1-3 ppm.

LRMS

BG_8B.d.zip BG_8B.pdf

KlementineJBS commented 1 year ago

IR

BG_8B.pdf

KlementineJBS commented 1 year ago

NMR

20221108_BG_8B_2.zip 20221108_BG_8B_1.zip

20221108_BG_8B proton and carbon 500 MHz.pdf

13C NMR (126 MHz, DMSO) δ 159.76, 152.94, 152.60, 149.82, 149.43, 149.17, 137.85, 123.18, 120.45, 111.34, 110.91, 107.00.

1H NMR (500 MHz, DMSO-d6) δ 11.86 (s, 1H), 8.60 (dd, J = 14.9, 4.7 Hz, 2H), 8.00 (d, J = 7.8 Hz, 1H), 7.91 (t, J = 7.6 Hz, 1H), 7.43 (s, 1H), 7.38 – 7.32 (m, 1H), 7.26 (d, J = 5.1 Hz, 1H).