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KlementineJBS / USYD_PhD_ELN

This repository forms the electronic laboratory notebook (ELN)for Klementine Burrell-Sander's PhD's
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Breaking Good SSP compounds - 8J #38

Closed KlementineJBS closed 1 year ago

KlementineJBS commented 1 year ago

image

KlementineJBS commented 1 year ago

F1-7 - very dilute, probably not worth using F8-13 - impurities F14-35 - mostly clean F36-70 - some impurities at low ppm F71-104 - mostly clean

Will pool 14-35 and 71-104.

KlementineJBS commented 1 year ago

IR

BG_8J.pdf

KlementineJBS commented 1 year ago

NMR

20221108_BG_8J_2.zip 20221108_BG_8J_1.zip

20221108_BG_8J proton and carbon 500 MHz.pdf

13C NMR (126 MHz, DMSO) δ 160.65, 152.25, 149.16, 146.92, 146.56, 141.30, 126.81, 124.58, 118.16, 111.17, 21.19.

1H NMR (500 MHz, DMSO-d6) δ 11.47 (s, 1H), 8.30 (d, J = 8.5 Hz, 2H), 8.18 (dd, J = 10.9, 7.0 Hz, 3H), 7.79 (s, 1H), 6.91 (s, 1H), 6.80 (s, 1H), 3.35 (s, 1H), 2.31 (s, 3H).