Stanford-ChEMH-MCAC / protocols

Laboratory protocols used by the Metabolite Chemistry Analysis Center, a ChEM-H Knowledge Center at Stanford University.
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procedure clean-up #35

Open wdwvt1 opened 4 years ago

wdwvt1 commented 4 years ago

A couple to-dos:

wdwvt1 commented 4 years ago

e.g. adding this from Qi and Amita 1.) Turn of all modules on screen. 2.) Open mass spec cover (temp may be hot). Wipe with EtOh spray bottle above mass spec. 3.) Close MassHunter. Remove Mass Hunter Process (from Windows search. 4.) Turn off IP-LC pump, autosampler, column. 5.) Disconnect "plug 2" from I-P LC and replug into "normal LC" 6.) Disconnect Plug 1 from I-P LC and replug into "normal LC" 7.) Remove wire from IP LC to MS and reconnect the other "normal LC" to the MS. 8.) Turn on "normal LC" pump, autosampler, column. Adjust waste tubes if needed. 9.) Wash for 6-8 hrs with 40% H20, 50% isopropanol, 10% acetic acid using ion pair cleaning method 20190314